The Avengers #3
In "The Avengers Meet... Sub-Mariner!", the team grapples with the fallout of the Hulk’s departure, only to face him again—this time in conflict. When the Sub-Mariner learns of the Hulk’s presence, an unlikely alliance forms between the two giants against their former foes. Written by Stan Lee and Jack Kirby, with art by Jack Kirby and inks by Paul Reinman, this pivotal 1964 issue features a cover by Jack Kirby and Paul Reinman.
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The Avengers feel responsible for the danger the Hulk may cause after he left the team in the previous issue. When they find the green Goliath a battle ensues. The Sub-Mariner learns of the Hulk's presence and after initially fighting each other Namor convinces the Hulk to join forces with him against the Avengers.
Plot details indexed by the Grand Comics Database (CC BY-SA).